9JVI

Crystal structure of OsSPS3 complexed with YH24288

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL10U2
Synchrotron site	SSRF
Beamline	BL10U2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-05-19
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.979183
Spacegroup name	P 21 21 21
Unit cell lengths	56.604, 90.356, 128.530
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	36.959 - 1.677
R-factor	0.1975
Rwork	0.196
R-free	0.22740
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	0.743
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX ((1.16_3549: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	36.959	1.737
High resolution limit [Å]	1.677	1.677
Number of reflections	76132	7428
<I/σ(I)>	16.19
Completeness [%]	99.8
Redundancy	10.249
CC(1/2)	0.999	0.841

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291	PEG3350, Bis-Tris, Ammonium sulfate