9JGO
Structure of Pd ions bound to human heavy chain ferritin nanocage.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 HF |
| Temperature [K] | 93 |
| Detector technology | AREA DETECTOR |
| Collection date | 2022-06-22 |
| Detector | RIGAKU |
| Wavelength(s) | 1.5418 |
| Spacegroup name | F 4 3 2 |
| Unit cell lengths | 183.960, 183.960, 183.960 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 45.990 - 1.851 |
| Rwork | 0.179 |
| R-free | 0.19740 |
| Structure solution method | SAD |
| Data reduction software | iMOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHENIX |
| Refinement software | PHENIX (1.20) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 45.990 | 1.917 |
| High resolution limit [Å] | 1.851 | 1.851 |
| Rmerge | 0.090 | 0.439 |
| Number of reflections | 23326 | 2277 |
| <I/σ(I)> | 37.65 | |
| Completeness [%] | 99.7 | 99.91 |
| Redundancy | 39.9 | |
| CC(1/2) | 1.000 | 0.984 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | EVAPORATION | 283 | 2 M MgCl2, 0.1 M Bicine, pH 9.0 |
