9IQ8

Ankyrin-like protein, AnkB

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 5C (4A)
Synchrotron site	PAL/PLS
Beamline	5C (4A)
Temperature [K]	125
Detector technology	PIXEL
Collection date	2022-09-25
Detector	DECTRIS EIGER X 9M
Wavelength(s)	1.000
Spacegroup name	C 1 2 1
Unit cell lengths	90.080, 90.220, 78.990
Unit cell angles	90.00, 116.38, 90.00

Refinement procedure

Resolution	28.425 - 2.420
R-factor	0.2485
Rwork	0.247
R-free	0.28310
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.010
RMSD bond angle	1.195
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHENIX
Refinement software	PHENIX ((1.13_2998: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	28.425	2.507
High resolution limit [Å]	2.420	2.420
Number of reflections	21670	2158
<I/σ(I)>	5.42
Completeness [%]	99.8
Redundancy	6.9
CC(1/2)	0.986	0.796

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293.15	0.1M Bis-Tris pH 6.7, 0.005M Hexammine cobalt chloride, 31% (w/v) PEG 5000 MME