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9ICC

DNA POLYMERASE BETA (E.C.2.7.7.7)/DNA COMPLEX + 2'-DEOXYADENOSINE-5'-TRIPHOSPHATE, SOAKED IN THE PRESENCE OF DATP AND CRCL3

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RU200
Temperature [K]298
Detector technologyAREA DETECTOR
Collection date1995-03-29
DetectorSDMS
Spacegroup nameP 21 21 2
Unit cell lengths179.300, 57.603, 48.013
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution20.000 - 3.100
R-factor0.157

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Structure solution methodDIFFERENCE FOURIER
Starting model (for MR)8icb
RMSD bond length0.019
RMSD bond angle19.000

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Data reduction softwareSDMS
Data scaling softwareSDMS
Phasing softwareTNT (V. 5-D)
Refinement softwareTNT (5-D)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]20.0003.200
High resolution limit [Å]3.1003.100
Rmerge0.065

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0.179

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Number of reflections8833
Completeness [%]92.092
Redundancy21.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Vapor diffusion, sitting drop

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6.5298

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THIS ENTRY DESCRIBES THE STRUCTURE THAT RESULTED WHEN A COCRYSTAL OF HUMAN DNA POLYMERASE BETA COMPLEXED WITH 7 BASE PAIRS OF DNA (SEE ENTRY 9ICJ AND REFERENCE 1) HAD BEEN SOAKED IN THE FOLLOWING SOLUTION FOR 24 HOURS: PEG 3350, 16% MES, 100 MILLIMOLAR, PH 6.5 NACL, 150 MILLIMOLAR DATP, 1 MILLIMOLAR CRCL3, 5 MILLIMOLAR SEE REFERENCE 2 FOR DETAILS CONCERNING EXPERIMENTAL PROCEDURES, RESULTS, AND DISCUSSION FOR THIS STRUCTURE.
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11reservoirPEG335015-17 (%)
21reservoircitrate0.1 (M)
31reservoir50 (mM)

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