9IA8

Crystal Structure of UFC1 K108R

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-08-11
Detector	DECTRIS PILATUS 200K
Wavelength(s)	1.54187
Spacegroup name	P 41 21 2
Unit cell lengths	47.010, 47.010, 142.150
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	44.630 - 1.900
Rwork	0.205
R-free	0.24750
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	1.483
Data reduction software	XDS
Data scaling software	XSCALE
Refinement software	REFMAC (5.8.0267)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	44.630	1.950
High resolution limit [Å]	1.900	1.900
Number of reflections	13433	971
<I/σ(I)>	8.52
Completeness [%]	96.8	100
Redundancy	1.2
CC(1/2)	0.990	0.474

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	5.5	298	0.1M Bis-Tris pH 5.5, 2M Ammonium Sulfate