Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-12-20 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.95374 |
| Spacegroup name | P 1 |
| Unit cell lengths | 36.095, 41.391, 45.815 |
| Unit cell angles | 90.12, 108.08, 106.17 |
Refinement procedure
| Resolution | 17.720 - 1.489 |
| R-factor | 0.2121 |
| Rwork | 0.211 |
| R-free | 0.23360 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.020 |
| Data reduction software | autoPROC |
| Data scaling software | autoPROC |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.11.8) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 39.567 | 1.624 |
| High resolution limit [Å] | 1.489 | 1.489 |
| Number of reflections | 27487 | 1375 |
| <I/σ(I)> | 7.7 | |
| Completeness [%] | 80.8 | |
| Redundancy | 1.8 | |
| CC(1/2) | 0.999 | 0.864 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 8 % PEG3350, 0.1 M PCTP buffer pH 4.5 |
