Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ELETTRA BEAMLINE 11.2C |
| Synchrotron site | ELETTRA |
| Beamline | 11.2C |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2023-11-22 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1.000 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 58.077, 45.855, 62.606 |
| Unit cell angles | 90.00, 111.23, 90.00 |
Refinement procedure
| Resolution | 49.653 - 2.000 |
| R-factor | 0.1684 |
| Rwork | 0.166 |
| R-free | 0.22330 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.864 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 58.360 | 2.050 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.088 | 0.879 |
| Rmeas | 0.097 | 0.963 |
| Rpim | 0.040 | 0.388 |
| Total number of observations | 122464 | 8943 |
| Number of reflections | 20975 | 1516 |
| <I/σ(I)> | 11.7 | 2.3 |
| Completeness [%] | 99.9 | |
| Redundancy | 5.8 | 5.9 |
| CC(1/2) | 0.998 | 0.746 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 32% PEG4000, 0.2 M Lithium Sulfate |
