9HRZ

The RSL-R6 - pctx complex, H3 form

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SOLEIL BEAMLINE PROXIMA 2
Synchrotron site	SOLEIL
Beamline	PROXIMA 2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-10-26
Detector	DECTRIS EIGER X 9M
Wavelength(s)	0.98
Spacegroup name	H 3
Unit cell lengths	43.569, 43.569, 122.997
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	18.650 - 1.490
R-factor	0.1729
Rwork	0.172
R-free	0.20280
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	1.301
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX ((1.20.1_4487))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	18.650	1.520
High resolution limit [Å]	1.490	1.490
Rmerge	0.051	0.276
Rmeas	0.054	0.297
Rpim	0.071	0.106
Number of reflections	14063	4873
<I/σ(I)>	25.6	5.2
Completeness [%]	99.6	94.2
Redundancy	10.3
CC(1/2)	0.999	0.983

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	0.8 M ammonium sulfate, 0.1 M sodium acetate pH 5.6