Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID30B |
| Synchrotron site | ESRF |
| Beamline | ID30B |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2023-04-21 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9697 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 128.326, 128.326, 124.563 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 42.630 - 2.400 |
| R-factor | 0.2126 |
| Rwork | 0.210 |
| R-free | 0.26160 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.014 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.19_4092: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 42.630 | 2.480 |
| High resolution limit [Å] | 2.400 | 2.400 |
| Number of reflections | 38876 | 4028 |
| <I/σ(I)> | 8.4 | |
| Completeness [%] | 94.0 | |
| Redundancy | 3.7 | |
| CC(1/2) | 0.996 | 0.894 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 33 % polyethylene glycol methyl ether 5000, 0.2 M ammonium sulfate, 0.1 MES pH 6.5 |
