Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-02-18 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.999996 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 92.820, 72.980, 52.430 |
| Unit cell angles | 90.00, 94.07, 90.00 |
Refinement procedure
| Resolution | 46.290 - 2.460 |
| R-factor | 0.2362 |
| Rwork | 0.234 |
| R-free | 0.26880 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.004 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.21rc1_5127: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 46.300 | 2.710 |
| High resolution limit [Å] | 2.460 | 2.460 |
| Rmerge | 0.066 | 0.990 |
| Rpim | 0.053 | 0.780 |
| Number of reflections | 12603 | 3116 |
| <I/σ(I)> | 7.4 | 0.9 |
| Completeness [%] | 98.7 | 98.6 |
| Redundancy | 2.3 | 2.3 |
| CC(1/2) | 0.997 | 0.550 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.2 | 293 | 0.2M CaCl2, 0.1 M Mops pH 6.2, 11-14% PEG8000, after microseeding |
