Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PETRA III, EMBL c/o DESY BEAMLINE P13 (MX1) |
| Synchrotron site | PETRA III, EMBL c/o DESY |
| Beamline | P13 (MX1) |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-11-08 |
| Detector | DECTRIS EIGER2 X CdTe 16M |
| Wavelength(s) | 0.97625 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 78.220, 78.220, 37.584 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 31.090 - 1.130 |
| R-factor | 0.1563 |
| Rwork | 0.156 |
| R-free | 0.16840 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.820 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.21rc1_5127) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 55.310 | 1.150 |
| High resolution limit [Å] | 1.130 | 1.130 |
| Rmerge | 0.037 | 0.415 |
| Rpim | 0.011 | 0.221 |
| Number of reflections | 42995 | 1351 |
| <I/σ(I)> | 43.2 | 4.1 |
| Completeness [%] | 97.9 | |
| Redundancy | 20 | |
| CC(1/2) | 1.000 | 0.910 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5 | 298 | 30% PEG 6000, 1 M NaCl, 50 mM sodium acetate |
