Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PETRA III, DESY BEAMLINE P11 |
| Synchrotron site | PETRA III, DESY |
| Beamline | P11 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-07-15 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1.033202 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 59.914, 74.950, 76.129 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 47.080 - 1.360 |
| R-factor | 0.1493 |
| Rwork | 0.148 |
| R-free | 0.16560 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.448 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.080 | 1.440 |
| High resolution limit [Å] | 1.360 | 1.360 |
| Rmerge | 0.078 | 0.853 |
| Rmeas | 0.083 | 0.895 |
| Rpim | 0.025 | 0.266 |
| Total number of observations | 776332 | 113983 |
| Number of reflections | 72913 | 10514 |
| <I/σ(I)> | 14.7 | 2.6 |
| Completeness [%] | 99.2 | |
| Redundancy | 10.6 | 10.8 |
| CC(1/2) | 0.999 | 0.863 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | JSCG+ condition F16: 0.1 M HEPES pH 7, 30% Jeff-M-600 |
