9GYJ

Vitamin D receptor in complex with Sila-c

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SOLEIL BEAMLINE PROXIMA 2
Synchrotron site	SOLEIL
Beamline	PROXIMA 2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-07-16
Detector	DECTRIS EIGER2 S 16M
Wavelength(s)	0.98
Spacegroup name	P 65 2 2
Unit cell lengths	65.745, 65.745, 262.744
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	47.740 - 1.900
R-factor	0.209
Rwork	0.208
R-free	0.23910
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	0.916
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHENIX
Refinement software	PHENIX ((1.17_3644: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.740	1.968
High resolution limit [Å]	1.900	1.900
Number of reflections	27676	2646
<I/σ(I)>	13.7
Completeness [%]	99.2
Redundancy	2
CC(1/2)	1.000	0.911

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	NaAcetate 2.5M