Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-05-19 |
| Detector | DECTRIS EIGER2 S 16M |
| Wavelength(s) | 0.99 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 225.274, 67.447, 136.880 |
| Unit cell angles | 90.00, 101.71, 90.00 |
Refinement procedure
| Resolution | 67.106 - 2.120 |
| Rwork | 0.218 |
| R-free | 0.25620 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.004 |
| RMSD bond angle | 1.391 |
| Data reduction software | autoPROC |
| Data scaling software | autoPROC |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 95.167 | 2.157 |
| High resolution limit [Å] | 2.120 | 2.120 |
| Rmerge | 0.159 | 1.178 |
| Number of reflections | 112044 | 5684 |
| <I/σ(I)> | 7.8 | |
| Completeness [%] | 97.8 | |
| Redundancy | 7.4 | |
| CC(1/2) | 0.989 | 0.460 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293 | MPD 50.0% v/v; NH4H2PO4 0.20M; Tris-HCL 0.10M pH 8.50 |
