9GT8
DTPAA CHIP EXPERIMENT, CRISTALLINA, X,Y SPACING 100,100
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | FREE ELECTRON LASER |
| Source details | SwissFEL ARAMIS BEAMLINE ESC |
| Synchrotron site | SwissFEL ARAMIS |
| Beamline | ESC |
| Temperature [K] | 293 |
| Detector technology | PIXEL |
| Collection date | 2023-06-01 |
| Detector | PSI JUNGFRAU 8M |
| Wavelength(s) | 1.030 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 72.600, 68.200, 73.900 |
| Unit cell angles | 90.00, 105.50, 90.00 |
Refinement procedure
| Resolution | 37.200 - 1.540 |
| R-factor | 0.16883 |
| Rwork | 0.168 |
| R-free | 0.19214 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.852 |
| Data reduction software | CrystFEL |
| Data scaling software | CrystFEL |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0430) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.000 | 1.580 |
| High resolution limit [Å] | 1.540 | 1.540 |
| Number of reflections | 102828 | 5104 |
| <I/σ(I)> | 5.6 | |
| Completeness [%] | 100.0 | |
| Redundancy | 638 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | BATCH MODE | 293 | PEG 6K, HEPES pH 7.0 |
