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9GON

Crystal structure of DPP9 in complex with sulphostin

This is a non-PDB format compatible entry.
Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X10SA
Synchrotron siteSLS
BeamlineX10SA
Temperature [K]100
Detector technologyPIXEL
Collection date2021-11-24
DetectorDECTRIS EIGER X 16M
Wavelength(s)0.9998
Spacegroup nameP 1
Unit cell lengths88.799, 106.683, 121.143
Unit cell angles65.05, 70.82, 76.58
Refinement procedure
Resolution90.210 - 1.890
R-factor0.16372
Rwork0.163
R-free0.20597
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.008
RMSD bond angle1.473
Data reduction softwareautoPROC
Data scaling softwareautoPROC ((Version 1.1.7))
Phasing softwarePHASER
Refinement softwareREFMAC (5.8.0267)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]90.2101.930
High resolution limit [Å]1.8901.890
Number of reflections28967414469
<I/σ(I)>5.3
Completeness [%]96.3
Redundancy2.2
CC(1/2)0.9900.960
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP29320% (w/v) PEG 2000 MME, 0.1M Tris pH 6.75

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