Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-11-24 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9998 |
Spacegroup name | P 1 |
Unit cell lengths | 88.799, 106.683, 121.143 |
Unit cell angles | 65.05, 70.82, 76.58 |
Refinement procedure
Resolution | 90.210 - 1.890 |
R-factor | 0.16372 |
Rwork | 0.163 |
R-free | 0.20597 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.473 |
Data reduction software | autoPROC |
Data scaling software | autoPROC ((Version 1.1.7)) |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 90.210 | 1.930 |
High resolution limit [Å] | 1.890 | 1.890 |
Number of reflections | 289674 | 14469 |
<I/σ(I)> | 5.3 | |
Completeness [%] | 96.3 | |
Redundancy | 2.2 | |
CC(1/2) | 0.990 | 0.960 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 20% (w/v) PEG 2000 MME, 0.1M Tris pH 6.75 |