Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 298 |
| Detector technology | PIXEL |
| Collection date | 2022-12-22 |
| Detector | DECTRIS PILATUS 200K |
| Wavelength(s) | 1.54187 |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 46.590, 46.590, 142.540 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 35.630 - 2.000 |
| Rwork | 0.177 |
| R-free | 0.23100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.584 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 35.630 | 2.072 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmeas | 0.098 | 0.730 |
| Number of reflections | 20248 | 1501 |
| <I/σ(I)> | 13.77 | 1.77 |
| Completeness [%] | 100.0 | 99.8 |
| Redundancy | 6.73 | 3.6 |
| CC(1/2) | 0.999 | 0.730 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 1.5M Ammonium sulfate, 0.1M Tris pH 8.0. |
