Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID30B |
| Synchrotron site | ESRF |
| Beamline | ID30B |
| Temperature [K] | 298 |
| Detector technology | PIXEL |
| Collection date | 2021-07-18 |
| Detector | DECTRIS EIGER X 9M |
| Wavelength(s) | 0.91976 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 41.653, 48.002, 82.580 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 29.399 - 1.350 |
| Rwork | 0.182 |
| R-free | 0.20100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.846 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.400 | 1.398 |
| High resolution limit [Å] | 1.350 | 1.350 |
| Rmeas | 0.066 | 1.179 |
| Number of reflections | 36233 | 3493 |
| <I/σ(I)> | 7.8 | 0.86 |
| Completeness [%] | 97.4 | 96.09 |
| Redundancy | 1.83 | 3 |
| CC(1/2) | 0.997 | 0.467 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 1.5M Ammonium sulfate, 0.1M Bis-Tris Propane pH 7.0 |
