9GLP

Crystal Structure of UFC1 C116E&T106I

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID23-2
Synchrotron site	ESRF
Beamline	ID23-2
Temperature [K]	298
Detector technology	PIXEL
Collection date	2024-01-19
Detector	DECTRIS EIGER X 9M
Wavelength(s)	0.87313
Spacegroup name	P 41 21 2
Unit cell lengths	46.837, 46.837, 144.089
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	44.543 - 1.770
Rwork	0.178
R-free	0.19960
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.011
RMSD bond angle	1.647
Refinement software	REFMAC (5.8.0267)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	44.543	1.833
High resolution limit [Å]	1.700	1.770
Rmeas	0.041	0.242
Number of reflections	16486	1605
<I/σ(I)>	13.74	3.44
Completeness [%]	100.0	100
Redundancy	2	2
CC(1/2)	0.999	0.924

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	5.5	293	0.1 M Bis-Tris, pH 5.5, 2 M ammonium sulfate.