Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 298 |
| Detector technology | PIXEL |
| Collection date | 2024-08-24 |
| Detector | DECTRIS PILATUS 200K |
| Wavelength(s) | 1.54187 |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 46.950, 46.950, 143.900 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 35.970 - 1.790 |
| Rwork | 0.192 |
| R-free | 0.23800 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.536 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 35.970 | 1.854 |
| High resolution limit [Å] | 1.790 | 1.790 |
| Rmeas | 0.039 | 0.352 |
| Number of reflections | 15997 | 1549 |
| <I/σ(I)> | 18.78 | 2.62 |
| Completeness [%] | 99.9 | 99.94 |
| Redundancy | 2 | 2 |
| CC(1/2) | 1.000 | 0.829 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 1.5M Ammonium sulfate; 0.1M Bis-Tris propane pH 7.0 |
