Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-12-14 |
| Detector | DECTRIS EIGER2 X 16M |
| Wavelength(s) | 0.9995 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 98.150, 81.226, 51.732 |
| Unit cell angles | 90.00, 114.78, 90.00 |
Refinement procedure
| Resolution | 47.010 - 1.476 |
| R-factor | 0.1386 |
| Rwork | 0.135 |
| R-free | 0.17690 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.388 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.010 | 1.500 |
| High resolution limit [Å] | 1.470 | 1.470 |
| Rmerge | 0.056 | |
| Number of reflections | 261893 | 13119 |
| <I/σ(I)> | 10.1 | |
| Completeness [%] | 96.1 | |
| Redundancy | 4.5 | |
| CC(1/2) | 0.824 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 293 | PCB: 0.100000 M pH:6.00 ; PEG 1500: 25.000000 %w/v |
