Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SOLEIL BEAMLINE PROXIMA 1 |
| Synchrotron site | SOLEIL |
| Beamline | PROXIMA 1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-09-12 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.978566 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 39.565, 109.557, 58.713 |
| Unit cell angles | 90.00, 96.97, 90.00 |
Refinement procedure
| Resolution | 34.570 - 1.841 |
| R-factor | 0.2023 |
| Rwork | 0.200 |
| R-free | 0.23940 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.900 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.10.4) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 34.570 | 1.940 |
| High resolution limit [Å] | 1.840 | 1.840 |
| Rmerge | 0.071 | 0.568 |
| Number of reflections | 224410 | 11910 |
| <I/σ(I)> | 8.53 | |
| Completeness [%] | 99.2 | 98 |
| Redundancy | 2.64 | 2.49 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 290 | Ammonium Sulfate 2.5M + MES 0.1M pH5.5 |
