9GFI

hRAR alpha LBD-AM580 complex with staple peptide

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SOLEIL BEAMLINE PROXIMA 2
Synchrotron site	SOLEIL
Beamline	PROXIMA 2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2021-11-20
Detector	DECTRIS EIGER X 9M
Wavelength(s)	0.98
Spacegroup name	C 1 2 1
Unit cell lengths	87.510, 62.060, 49.350
Unit cell angles	90.00, 105.57, 90.00

Refinement procedure

Resolution	42.150 - 2.100
R-factor	0.2281
Rwork	0.223
R-free	0.27160
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	0.940
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	BUSTER (2.10.4)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	42.120	2.200
High resolution limit [Å]	2.100	2.100
Rmerge	0.087	0.356
Number of reflections	14960	1936
<I/σ(I)>	17.16
Completeness [%]	99.8
Redundancy	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		290	PEG 3350 20%, 0.2M NaSCN