Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | LIQUID ANODE |
| Source details | BRUKER METALJET |
| Temperature [K] | 193 |
| Detector technology | PIXEL |
| Collection date | 2024-02-01 |
| Detector | Bruker PHOTON II |
| Wavelength(s) | 1.541840 |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 87.185, 40.452, 55.746 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 17.170 - 1.712 |
| R-factor | 0.1824 |
| Rwork | 0.180 |
| R-free | 0.22300 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 0.980 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | DIMPLE |
| Refinement software | BUSTER (2.11.8) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 55.740 | 1.820 |
| High resolution limit [Å] | 1.710 | 1.710 |
| Number of reflections | 18748 | 937 |
| <I/σ(I)> | 11 | |
| Completeness [%] | 93.0 | |
| Redundancy | 3.9 | |
| CC(1/2) | 0.990 | 0.470 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 277 | 0.2 mM MgCl2, 15% PEG 2000, 100 mM sodium acetate pH 4.4 |
