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9G3B

Crystal Structure of the artificial protein METP in complex with cadmium ion at different temperature, 130 K

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsELETTRA BEAMLINE 5.2R
Synchrotron siteELETTRA
Beamline5.2R
Temperature [K]100
Detector technologyPIXEL
Collection date2000-01-01
DetectorDECTRIS PILATUS3 6M
Wavelength(s)0.534
Spacegroup nameC 2 2 21
Unit cell lengths34.419, 56.352, 19.148
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution29.370 - 1.900
R-factor0.1489
Rwork0.143
Structure solution methodSAD
RMSD bond length0.013
RMSD bond angle1.335
Data reduction softwareXDS
Data scaling softwareSCALA
Phasing softwarePHASER
Refinement softwarePHENIX (1.21_5207)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]29.3701.800
High resolution limit [Å]1.7001.700
Rmerge0.079
Number of reflections8740450
<I/σ(I)>8.82
Completeness [%]95.196.3
Redundancy2.2
CC(1/2)0.9950.903
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.5298drop containing 2.0 μL of 1:1 (v/v) mixture of protein solution (10 mg/mL, 7 mM DTT, 4 mM CdCl2) and 2.0 μL of precipitant buffer (0.1 M HEPES at pH 7.5, 1.4 M sodium citrate tribasic dihydrate) was equilibrated against 0.5 mL reservoir of precipitant buffer

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