9FZ4
SARS CoV-2 nsp10 in complex with theExoN domain from nsp14
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX IV BEAMLINE BioMAX |
Synchrotron site | MAX IV |
Beamline | BioMAX |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-10-15 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.976 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 62.034, 70.724, 109.205 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 53.940 - 2.440 |
R-factor | 0.1863 |
Rwork | 0.181 |
R-free | 0.22860 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.182 |
Data reduction software | autoPROC |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.18.2_3874: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 54.000 | 2.480 |
High resolution limit [Å] | 2.440 | 2.440 |
Rmerge | 0.200 | 0.123 |
Number of reflections | 18581 | 915 |
<I/σ(I)> | 12.1 | |
Completeness [%] | 100.0 | 100 |
Redundancy | 13 | |
CC(1/2) | 0.994 | 0.810 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293 | 0.04-0.24 M Amino acids, 0.1 M buffer system 2 (pH 7.5), 16-38% v/v precipitant mix 2. |