9FX5
Crystal structure of Cryo2RT Thaumatin at 296K
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 296 |
Detector technology | PIXEL |
Collection date | 2023-09-13 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 1 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 58.449, 58.449, 151.499 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.270 - 1.592 |
R-factor | 0.1944 |
Rwork | 0.193 |
R-free | 0.22120 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | IN HOUSE MODEL |
RMSD bond length | 0.010 |
RMSD bond angle | 1.040 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.4) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.280 | 1.690 |
High resolution limit [Å] | 1.590 | 1.590 |
Rmeas | 0.070 | 2.310 |
Number of reflections | 36150 | 5700 |
<I/σ(I)> | 27.46 | 1.15 |
Completeness [%] | 100.0 | 100 |
Redundancy | 26.15 | 26.67 |
CC(1/2) | 1.000 | 0.740 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 1.6M Na. K. Tartrate |