Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2011-11-10 |
| Detector | DECTRIS PILATUS 2M |
| Wavelength(s) | 1.00002 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 37.060, 44.390, 78.600 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 38.650 - 1.250 |
| R-factor | 0.1805 |
| Rwork | 0.180 |
| R-free | 0.19010 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.910 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | BUSTER |
| Refinement software | BUSTER (2.11.2) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 38.650 | 1.300 |
| High resolution limit [Å] | 1.250 | 1.250 |
| Rmeas | 4.700 | 18.200 |
| Number of reflections | 36386 | 3809 |
| <I/σ(I)> | 23.73 | |
| Completeness [%] | 99.3 | 95.2 |
| Redundancy | 6.07 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 16.5 % PEG 3350, 0.1 M sodium nitrate, 8 % ethylene glycol |
