9FSE

Human ROR2 cysteine-rich domain (CRD) and Kringle domain

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I03
Synchrotron site	Diamond
Beamline	I03
Temperature [K]	100
Detector technology	PIXEL
Collection date	2015-09-22
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.9763
Spacegroup name	P 32 2 1
Unit cell lengths	109.554, 109.554, 45.004
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	94.880 - 2.480
R-factor	0.2381
Rwork	0.236
R-free	0.27050
Structure solution method	SAD
RMSD bond length	0.002
RMSD bond angle	0.468
Data reduction software	autoPROC (20230726)
Phasing software	AutoSol
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	94.880	2.733
High resolution limit [Å]	2.480	2.484
Rmerge	0.079	1.057
Rpim	0.027	0.429
Number of reflections	7221	361
<I/σ(I)>	14	1.5
Completeness [%]	93.2	68.4
Redundancy	9.8	6.8
CC(1/2)	0.998	0.686

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7.5	298.15	0.1 M HEPES pH 7.5, 1.5 M LiSO4