9FAF
Human adenovirus type 36 fiber knob in complex with 4-O,5-N-diacetylneuraminic acid
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-02-14 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 59.457, 99.164, 110.987 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.426 - 1.760 |
R-factor | 0.166009324593 |
Rwork | 0.165 |
R-free | 0.18391 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.894 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.850 |
High resolution limit [Å] | 1.760 | 1.760 |
Number of reflections | 65546 | 9952 |
<I/σ(I)> | 14.5 | |
Completeness [%] | 99.0 | 94.1 |
Redundancy | 13.1 | |
CC(1/2) | 0.999 | 0.647 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 277 | 24% PEG 3350, 185 mM NH4Ac, 0,1 M Bis-Tris pH 5.5 |