Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2019-07-17 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.97950 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 62.902, 83.563, 91.527 |
| Unit cell angles | 90.00, 92.18, 90.00 |
Refinement procedure
| Resolution | 50.230 - 2.469 |
| R-factor | 0.307 |
| Rwork | 0.306 |
| R-free | 0.32560 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.960 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.11.8) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.230 | 2.530 |
| High resolution limit [Å] | 2.470 | 2.470 |
| Number of reflections | 34161 | 2525 |
| <I/σ(I)> | 7 | |
| Completeness [%] | 100.0 | |
| Redundancy | 3.4 | |
| CC(1/2) | 0.988 | 0.751 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 15 % PEG10K, pH 6.5 |
