9F9H
Laser excitation effects on BR: Reprocessed Extrapolated 10ps Light dataset recorded at 525 GW/cm2 from Nogly et al.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | FREE ELECTRON LASER |
| Source details | SLAC LCLS BEAMLINE CXI |
| Synchrotron site | SLAC LCLS |
| Beamline | CXI |
| Temperature [K] | 298 |
| Detector technology | PIXEL |
| Collection date | 2017-06-30 |
| Detector | CS-PAD CXI-1 |
| Wavelength(s) | 1.3 |
| Spacegroup name | P 63 |
| Unit cell lengths | 62.950, 62.950, 111.700 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 16.020 - 1.660 |
| R-factor | 0.2335 |
| Rwork | 0.231 |
| R-free | 0.26840 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.019 |
| RMSD bond angle | 1.586 |
| Data reduction software | CrystFEL (0.9.1) |
| Data scaling software | CrystFEL (0.9.1) |
| Refinement software | PHENIX ((1.20_4459: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 19.350 | 1.600 |
| High resolution limit [Å] | 1.550 | 1.550 |
| Number of reflections | 35453 | 3534 |
| <I/σ(I)> | 9.19 | 1.19 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 194 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | LIPIDIC CUBIC PHASE | 5.6 | 294 | 100 mM Na/K Phosphate buffer pH 5.6 30 % PEG 2000 |
