9F9F
Laser excitation effects on BR: Extrapolated 6 ps Light dataset recorded at 2493 GW/cm2 at SwissFEL
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | FREE ELECTRON LASER |
| Source details | SwissFEL ARAMIS BEAMLINE ESA |
| Synchrotron site | SwissFEL ARAMIS |
| Beamline | ESA |
| Temperature [K] | 293 |
| Detector technology | PIXEL |
| Collection date | 2018-12-08 |
| Detector | PSI JUNGFRAU 16M |
| Wavelength(s) | 1.028919 |
| Spacegroup name | P 63 |
| Unit cell lengths | 62.950, 62.950, 111.700 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 15.740 - 1.800 |
| R-factor | 0.2196 |
| Rwork | 0.216 |
| R-free | 0.25880 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.154 |
| Data reduction software | CrystFEL (0.9.1) |
| Data scaling software | CrystFEL (0.9.1) |
| Refinement software | PHENIX ((1.20_4459: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 16.020 | 1.710 |
| High resolution limit [Å] | 1.660 | 1.660 |
| Number of reflections | 29593 | 2938 |
| <I/σ(I)> | 9.94 | 1.1 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 235 | 155 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | LIPIDIC CUBIC PHASE | 293 | 100 mM Na/K Phosphate buffer pH 5.6 30 % PEG 2000 |
