9F9A

Crystal structure of MUS81-EME1 bound by compound 12.

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04
Synchrotron site	Diamond
Beamline	I04
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-03-04
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.91587
Spacegroup name	P 21 21 21
Unit cell lengths	111.869, 124.348, 217.571
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	83.166 - 2.911
R-factor	0.2447
Rwork	0.243
R-free	0.27820
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	0.920
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	BUSTER (2.11.8)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	83.166	3.226
High resolution limit [Å]	2.911	2.911
Number of reflections	40849	2042
<I/σ(I)>	9.3
Completeness [%]	94.6
Redundancy	6.7
CC(1/2)	0.999	0.720

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		297	20 % ethanol