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9F8W

Crystal structure of the apo Pex5 peroxisomal cargo receptor from Trypanosoma brucei

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsBESSY BEAMLINE 14.1
Synchrotron siteBESSY
Beamline14.1
Temperature [K]100
Detector technologyPIXEL
Collection date2019-11-10
DetectorDECTRIS PILATUS3 S 6M
Wavelength(s)0.9184
Spacegroup nameH 3
Unit cell lengths206.545, 206.545, 67.867
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution47.890 - 2.350
R-factor0.20025
Rwork0.198
R-free0.24605
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.008
RMSD bond angle1.552
Data reduction softwareXDS
Data scaling softwareAimless
Phasing softwarePHASER
Refinement softwareREFMAC (5.8.0267)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]47.8902.434
High resolution limit [Å]2.3502.350
Number of reflections449174490
<I/σ(I)>14.68
Completeness [%]99.9
Redundancy5.86
CC(1/2)0.9990.520
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7.42930.9 M sodium-potassium tartrate tetrahydrate, 20% w/v glycerol, 0.05 M Hepes pH 7.4 after 8 days at 293 K

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