9F8G
Photostatin (photoswitchable azo-combretastatin) Z-PST27 bound to tubulin-DARPin D1 complex
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-02-25 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 73.460, 91.115, 82.684 |
Unit cell angles | 90.00, 97.61, 90.00 |
Refinement procedure
Resolution | 44.620 - 2.200 |
R-factor | 0.1883 |
Rwork | 0.187 |
R-free | 0.22560 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.610 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.14-3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.620 | 2.032 |
High resolution limit [Å] | 1.905 | 1.905 |
Rmerge | 0.135 | 0.720 |
Rmeas | 0.148 | 0.846 |
Rpim | 0.059 | 0.439 |
Number of reflections | 65942 | 3297 |
<I/σ(I)> | 13.385 | 1.837 |
Completeness [%] | 78.2 | 22.34 |
Redundancy | 6.13 | 3.69 |
CC(1/2) | 0.990 | 0.697 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | 21% PEG 3000 (w/v), 0.2 M ammonium sulfate and 0.1 M bis-tris methane |