Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-09-03 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.99999 |
| Spacegroup name | P 41 |
| Unit cell lengths | 74.587, 74.587, 97.035 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 46.380 - 2.700 |
| R-factor | 0.20583 |
| Rwork | 0.203 |
| R-free | 0.26833 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.352 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0419) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.520 | 2.830 |
| High resolution limit [Å] | 2.700 | 2.700 |
| Number of reflections | 14673 | 1953 |
| <I/σ(I)> | 17.4 | |
| Completeness [%] | 100.0 | |
| Redundancy | 14 | |
| CC(1/2) | 0.999 | 0.760 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8 | 278 | 15% PEG 6k 0.1M bicine 8.0 |
