Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-12-16 |
| Detector | DECTRIS PILATUS 2M-F |
| Wavelength(s) | 1.00 |
| Spacegroup name | P 64 2 2 |
| Unit cell lengths | 113.382, 113.382, 213.926 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 49.100 - 2.402 |
| R-factor | 0.2612 |
| Rwork | 0.260 |
| R-free | 0.28960 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.840 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.11.8) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.100 | 2.550 |
| High resolution limit [Å] | 2.400 | 2.400 |
| Rmeas | 0.241 | 5.360 |
| Number of reflections | 59933 | 9642 |
| <I/σ(I)> | 9.81 | 0.59 |
| Completeness [%] | 99.9 | |
| Redundancy | 10.6 | |
| CC(1/2) | 1.000 | 0.426 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 1.0M NaMalonate pH 5.0, 0.1M NaAcetate pH 4.50, 2% PEG 20,000 |
