Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-10-20 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1.00 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 84.245, 92.135, 132.329 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.070 - 2.249 |
R-factor | 0.2405 |
Rwork | 0.239 |
R-free | 0.27150 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.870 |
Data reduction software | autoPROC |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.8) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.100 | 2.390 |
High resolution limit [Å] | 2.250 | 2.250 |
Rmeas | 0.134 | 1.600 |
Number of reflections | 94264 | 15079 |
<I/σ(I)> | 9.3 | 0.84 |
Completeness [%] | 99.6 | |
Redundancy | 3.5 | |
CC(1/2) | 0.997 | 0.400 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 10% w/v PEG 4000, 20% v/v glycerol, 0.1 M MOPS/HEPES-Na pH 7.5 |