9EQP

N-terminal domain of Infectious Bursal Disease Virus (IBDV) VP3

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID30B
Synchrotron site	ESRF
Beamline	ID30B
Temperature [K]	100
Detector technology	PIXEL
Collection date	2016-07-06
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.9686
Spacegroup name	P 21 21 21
Unit cell lengths	50.687, 111.416, 277.012
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	47.600 - 3.500
R-factor	0.2392
Rwork	0.238
R-free	0.25910
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	0.859
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	MOLREP
Refinement software	PHENIX ((dev_4788: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.600	3.680
High resolution limit [Å]	3.500	3.500
Rmerge	0.187	1.237
Rmeas	0.209	1.382
Rpim	0.091	0.596
Number of reflections	19960	4736
<I/σ(I)>	8.17
Completeness [%]	97.6	98.2
Redundancy	4.7	4.8
CC(1/2)	0.992	0.529

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	8	293.15	0.8 M LiSO4, 0.05 M Sodium Cacodylate pH6.0