9EQO

N-terminal domain Infectious Bursal Disease Virus (IBDV) VP3

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALBA BEAMLINE XALOC
Synchrotron site	ALBA
Beamline	XALOC
Temperature [K]	100
Detector technology	PIXEL
Collection date	2015-10-29
Detector	DECTRIS PILATUS 6M
Wavelength(s)	1.0396
Spacegroup name	P 32 2 1
Unit cell lengths	54.952, 54.952, 89.468
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	47.590 - 1.340
R-factor	0.1623
Rwork	0.162
R-free	0.17290
Structure solution method	AB INITIO PHASING
RMSD bond length	0.007
RMSD bond angle	0.980
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	Arcimboldo
Refinement software	PHENIX ((dev_4788: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.590	1.380
High resolution limit [Å]	1.340	1.340
Rmerge	0.056	0.965
Rmeas	0.058	0.918
Rpim	0.013	0.329
Number of reflections	35270	20955
<I/σ(I)>	22.1	1.5
Completeness [%]	98.6
Redundancy	17.5
CC(1/2)	0.999	0.815

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	8	293.15	1.5M NaCl, 0.1M Sodium Acetate pH4.5