Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2023-07-07 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.99986 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 74.901, 74.901, 61.146 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 47.367 - 2.900 |
| R-factor | 0.224 |
| Rwork | 0.222 |
| R-free | 0.25410 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.562 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.12rc1_2801: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.370 | 3.000 |
| High resolution limit [Å] | 2.900 | 2.900 |
| Rpim | 0.134 | 1.050 |
| Number of reflections | 4177 | 416 |
| <I/σ(I)> | 8 | 0.5 |
| Completeness [%] | 99.6 | 99 |
| Redundancy | 25 | 26.7 |
| CC(1/2) | 0.994 | 0.440 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2M MgCl2, 0.1m Hepes 7.5, 30% Isopropanol |
