Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-08-09 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1.00003 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 103.861, 59.866, 75.227 |
| Unit cell angles | 90.00, 91.39, 90.00 |
Refinement procedure
| Resolution | 51.915 - 1.900 |
| R-factor | 0.1606 |
| Rwork | 0.159 |
| R-free | 0.19360 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 51.915 | 1.940 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Rpim | 0.080 | 0.821 |
| Number of reflections | 36026 | 2045 |
| <I/σ(I)> | 7.2 | |
| Completeness [%] | 98.3 | 86.3 |
| Redundancy | 12.7 | 8.7 |
| CC(1/2) | 0.986 | 0.529 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M Succinic acid pH 7.0, 15% w/v Polyethylene glycol 3,350 |
