Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-06-25 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.999999 |
| Spacegroup name | P 3 2 1 |
| Unit cell lengths | 59.290, 59.290, 74.295 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 51.347 - 1.800 |
| R-factor | 0.1686 |
| Rwork | 0.167 |
| R-free | 0.19700 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 51.350 | 1.864 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Rmerge | 0.349 | 1.511 |
| Rpim | 0.080 | 0.354 |
| Number of reflections | 14473 | 1428 |
| <I/σ(I)> | 15.9 | 1 |
| Completeness [%] | 99.8 | 99.9 |
| Redundancy | 19.1 | 18.8 |
| CC(1/2) | 0.971 | 0.630 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.15M KCl, 0.1M Hepes7.6, 14% PEG5000MME |
