9EM4
OPR3 variant Y364P in its dimeric form obtained with ammonium sulfate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID30B |
Synchrotron site | ESRF |
Beamline | ID30B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2024-02-08 |
Detector | DECTRIS EIGER2 X 9M |
Wavelength(s) | 0.87 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 57.531, 89.640, 80.943 |
Unit cell angles | 90.00, 109.01, 90.00 |
Refinement procedure
Resolution | 46.500 - 2.010 |
R-factor | 0.2081 |
Rwork | 0.206 |
R-free | 0.24380 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.014 |
RMSD bond angle | 0.742 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.21_5207: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.500 | 2.050 |
High resolution limit [Å] | 2.010 | 2.010 |
Rpim | 0.050 | 0.630 |
Number of reflections | 51254 | 2515 |
<I/σ(I)> | 9.09 | |
Completeness [%] | 99.3 | |
Redundancy | 6.9 | |
CC(1/2) | 0.990 | 0.530 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.1 M MES/Tris (6.5), 10 mM ammonium sulfate, 8-16% PEG8000 |