9EM3
OPR3 wild type in its monomeric form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID30B |
Synchrotron site | ESRF |
Beamline | ID30B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2024-02-08 |
Detector | DECTRIS EIGER2 X 9M |
Wavelength(s) | 0.8731 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 87.260, 89.840, 48.880 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.940 - 2.270 |
R-factor | 0.2153 |
Rwork | 0.213 |
R-free | 0.26150 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.751 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.21_5207) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.940 | 2.410 |
High resolution limit [Å] | 2.270 | 2.270 |
Rpim | 0.250 | 1.270 |
Number of reflections | 48983 | 8108 |
<I/σ(I)> | 2.72 | |
Completeness [%] | 97.5 | |
Redundancy | 3 | |
CC(1/2) | 0.950 | 0.190 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.1 M MES/Tris (6.5), 10 mM ammonium sulfate, 8-16% PEG8000 |