9EM0
OPR3 wild type in its dimeric form with special L6 conformation
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID30B |
Synchrotron site | ESRF |
Beamline | ID30B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2024-02-08 |
Detector | DECTRIS EIGER2 X 9M |
Wavelength(s) | 0.8731 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 57.695, 89.659, 80.148 |
Unit cell angles | 90.00, 104.17, 90.00 |
Refinement procedure
Resolution | 47.460 - 2.200 |
R-factor | 0.2496 |
Rwork | 0.249 |
R-free | 0.27680 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.002 |
RMSD bond angle | 0.460 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.21_5207) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.460 | 2.090 |
High resolution limit [Å] | 1.990 | 1.990 |
Rpim | 0.230 | 1.710 |
Number of reflections | 102435 | 10325 |
<I/σ(I)> | 2.47 | |
Completeness [%] | 97.2 | |
Redundancy | 3.4 | |
CC(1/2) | 0.960 | 0.150 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M MES/Tris (6.5), 50 mM ammonium sulfate, 16% PEG8000 |