9EFY

Co-MAHF-9 A8G Metal Alpha-Helix Framework

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	MAX IV BEAMLINE BioMAX
Synchrotron site	MAX IV
Beamline	BioMAX
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-05-08
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.68880
Spacegroup name	P 1
Unit cell lengths	10.320, 16.240, 21.570
Unit cell angles	67.92, 89.37, 71.85

Refinement procedure

Resolution	14.560 - 0.910
R-factor	0.1824
Rwork	0.180
R-free	0.20690
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	1.542
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	14.560	0.940
High resolution limit [Å]	0.910	0.910
Number of reflections	24651	172
<I/σ(I)>	3.95
Completeness [%]	92.6
Redundancy	2.6
CC(1/2)	0.993	0.025

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	SLOW COOLING		298	water, acetonitrile, cobalt acetate
1	SLOW COOLING		298	water, acetonitrile, cobalt acetate