9EA8
Citrobacter BubCD(D104A)-BubA(155-229) complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2024-04-13 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97946 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 96.636, 96.636, 135.204 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.310 - 2.340 |
R-factor | 0.2393 |
Rwork | 0.238 |
R-free | 0.26820 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.611 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.21.1_5286) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.310 | 2.420 |
High resolution limit [Å] | 2.340 | 2.340 |
Rmerge | 0.060 | 1.634 |
Number of reflections | 27750 | 2663 |
<I/σ(I)> | 25.8 | 1.7 |
Completeness [%] | 100.0 | |
Redundancy | 13.4 | |
CC(1/2) | 1.000 | 0.720 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 100 mM MES pH 6.0, 2.2 M sodium acetate pH 7.0 |