9DMR

Solution NMR structure of the calcium insensitive human LETM1 F-EF-hand domain mutant in the absence of calcium

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Varian	INOVA		600

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
2	1	1	3D 1H-15N NOESY
3	1	2	3D CBCA(CO)NH
4	1	2	3D HNCACB
5	1	2	3D H(CCO)NH
6	1	2	3D HNCO
7	2	3	2D 1H-13C HSQC
8	2	3	3D HCCH-TOCSY
9	2	3	3D 1H-13C NOESY

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	7.8	1	308.15
2	8.2	1	308.15

Conformers

Conformers Calculated Total Number	200
Conformers Submitted Total Number	10